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Publikationstyp
Wissenschaftlicher Artikel
Erscheinungsjahr
2019
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Development and testing of a fractionated filtration for sampling of microplastics in water

Herausgeber
Quelle
Water Research
149 (2019)
Schlagwörter
Probenahme, Wasser
Zitation
BANNICK, Claus Gerhard, Nathan OBERMAIER, Mathias RICKING, Sara SCHNIEGLER und Regine SZEWZYK, 2019. Development and testing of a fractionated filtration for sampling of microplastics in water. Water Research [online]. 2019. Bd. 149 (2019). DOI 10.60810/openumwelt-1230. Verfügbar unter: https://openumwelt.de/handle/123456789/5934
Zusammenfassung englisch
A harmonization of sampling, sample preparation and detection is pivotal in order to obtain comparable data on microplastics (MP) in the environment. This paper develops and proposes a suitable sampling concept for waterbodies that considers different plastic specific properties and influencing factors in the environment. Both artificial water including defined MP fractions and the discharge of a wastewater treatment plant were used to verify the derived sampling procedure, sample preparation and the subsequent analysis of MP using thermal extraction-desorption gas chromatography - mass spectrometry (TED-GC-MS). A major finding of this paper is that an application of various particle size classes greatly improves the practical handling of the sampling equipment. Size classes also enable the TED-GC-MS to provide any data on the MP size distribution, a substantial sampling property affecting both the necessary sampling volume and the optimal sampling depth. In the artificial body of water with defined MP fractions, the recovery rates ranged from 80-110%, depending on the different MP types and MP size classes. In the wastewater discharge, we found both polyethylene and polystyrene in different size classes and quantities. © 2018 Elsevier Ltd. All rights reserved.